900: 5mm PATXI, Z568801/0009

1. General Information
2. Hard Pulses
3. Soft Pulses
4. Miscellaneous
5. Conditions for pulse determination:

In principle: Do NOT trust these values blindly - verify them if questionable!

Amplifiers can go bad or your sample environment like salt, temperature, ... might alter the pulse width!

1. General Information:

Shimfile: 568801_0009ws.shim is a good starting point for aqueous samples

Read Pulses from Master List:

Read in pulse sequence and Parameter file
Use the getprosol command or click on the test tube symbol in ased
For Bruker Pulse Sequences type: getprosol 1H 'p1' ' pldb1' , where p1 is the determined pulse length [us] at the power level PldB1 [dB].

2. Hard Pulses:

Nucleus	Type	Attenuation[dB]	Channel	90deg Pulse	Power[W]	Calc.	Date
1H		-13.0 dB	f1	7.80 us	20W		08/18/11
	waltz16		f1	70.0 us
	TOCSY		f1	24 us
	ROESY		f1	80.0 us
					.
13C	hard	-24.40 dB	f2	12.0 us	275.4 W		08/18/11
AcGly	TOCSY	-18.50 dB	f2	24.0 us	70.80 W	dB	08/18/11
AcGly	bilev cpd	-18.15 dB	f2	25.0 us	65.31 W	dB	08/18/11
	2nd cpd pg	-9.10 dB	f2	71.0 us	8.13 W	dB	08/18/11
	cpd	-12.15 dB	f2	50.0 us	16.40 W	dB	08/18/11
	LowDec 1	-6.10 dB	f2	100.0 us	4.07 W	dB	08/18/11
					.
15N	hard	-24.80 dB	f3	35.0 us	302.0 W		08/18/11
		-17.55dB	f3	84.0 us	56.89W	-17.20dB	08/18/11
		-10.30dB	f3	190.0 us	10.72W	-10.11dB	08/18/11
					.
2H		-19.95 dB	f1	170.0 us	60.0 W		08/17/11
AcGly		dB	f1	250 us	W		08/17/11

3. Soft Pulses:

Nucleus	Type	Channel	Pulse	Attenuation [dB]	Power [W]	Resonance	Date
13C , Cali/CO	Q5.1000 213us	f2	90 deg	-24.60 dB	288.4 W	on	08/19/11
Cali/CO	Q5tr.1000 213us	f2	90 deg	-24.65 dB	291.74 W	on	08/19/11
Cali/CO	Q5.1000 1000us	f2	90 deg	-11.20 dB	13.18 W	on	08/19/11
Cali/CO	Q5tr.1000 1000us	f2	90 deg	-11.45 dB	13.96 W	on	08/19/11
Cali/CO	Q3.1000 170us	f2	180 deg	-23.75 dB	237.14 W	on	08/19/11
Cali/CO	Q3.1000 170us	f2	180 deg	-23.75 dB	237.14 W	off(-136ppm)	08/19/11
CO	Q3.1000 467us	f2	180 deg	-15.00 dB	31.62 W	on	08/19/11
CO	Q3.1000 667us	f2	180 deg	-12.00 dB	15.85 W	on	08/19/11
Cα	Q3.1000 1333us	f2	180 deg	-5.85 dB	3.85 W	on	08/19/11

4. Miscellaneous:

Offset Ca - carbonyl (56 - 175ppm):	-26936Hz
1H offset @ 4.7 pppm:	4230.94 Hz
Main Field:	900.20 MHz
BSMS Field:	+762 units (08-19-2011)

5. Conditions for pulse determination:

Samples:
1H-pulses: 2mM Sucrose + 0.5mM DSS + 2mM NaN3, 90% H2O 10% D2O
X-pulses: 13C, 15N labled Urea in DMSO
13C-shift: 48.5ppm, J=138.5Hz
15N-shift: 76.0ppm, J=88.5Hz
Temperature: 298K